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Friday, November 15, 2013

Gravimetric determination of water in hydrated magnesium chloride

Aim: To calculate the value of n in MgCl2.nH2O guess: Gravimetric summary is where the amount of a specific chemic in a matteerial is determined by converting it to a product which set up be isolated all and weighed. This is relevant to this experiment as the amount of water is an hidden value which is to be name by carrying let out the analysis. thawing to constant chew is when repeated estrus, chilling soce weighing is carried out until the plentifulness of the substance is constant. The outlet of moles of water in a substance can be found by measurement the loss in mass on hotness. MgCl2.nH2O MgCl2.nH2O n can be calculated by study the mass of hydrated gross salt with the mass of anhydrous salt by heating to constant mass. Apparatus: The equipment required is: a porcelain melting throne and lid tripod pipe-clay triangle bunsen burner and heating mat desiccator tongs a balance hydrated barium chloride. mode: To get rid of any water the crucib le was heated, and so allowed to assuredness in a desiccator and its mass was renowned (M1). 2-3g of milligram chloride was then added and the crucible reweighed (M2). The crucible and its contents were then reheated for 15 minutes, allowed to cool and again weighed (M3).
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The crucible and its contents were then heated, allowed to cool and weighed again, (M4), to make sure the loss in mass was complete. This look was repeated until M4 and M5 were constant. Results: M1 = 39.59g M2 = 41.62g M3 = 40.64g M4 = 40.63g Average mass of crucible and anhydrous MgCl2 = 40.635 great deal of anhydrous MgCl2 (M4 - M1) = 1.045g physiqu! e of moles of MgCl2 (GFM = 95.3g) = 1.045/95.3 = 0.012moles Mass of H2O removed M2 - M4 = 0.985g Number of moles of H2O (GFM... If you want to get a full essay, coordinate it on our website: OrderCustomPaper.com

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